On-line Fixed-Bed Microflow Reactor System Equiped with Shimazu GC-2014 (Micro-Scale)

Specifications for GC

Column Oven
Temperature Range	(Ambient + 10°C) ~ 400°C (using liquid CO₂ gas: -50°C - 400°C)
Dimensions	250 (W) x 360 (H) x 175 (D) mm
Oven Capacity	15.8L
Temperature Accuracy	Set value (K) ±1% (calibration at 0.01°C increments)
Temperature Deviation	2°C max. (on 200mm dia. circumfrence 30 mm from rear)
Temperature Variation Coefficient	0.01°C/°C
Temperature Program Steps	Up to 20 (cooling program possible)
Programmed rate setting range	-250°C ~ 250°C/min
Total time for all steps	9999.99 minutes max.
Linear Heating Range	30°C/min up to 150°C 20°C/min up to 250°C 10°C/min up to 380°C 7°C/min up to 400°C (at 25°C ambient temperature)
Cooling Rate	300°C ~ 50°C in 6 min max. (at 25°C ambient temperature)
Columns Accepted	Capillary Columns: 2 Packed columns for GC14B: 4 (Glass columns:2)

Sample Injection Unit
Temperature Range	Up to 400°C
Heating Settings	1°C steps
No. of units installed simultaneously	Up to 3 units
Sample injection unit types	Dual packed, single packed, split/splitless

Carrier Gas Flow Controller
For Packed/Dual
Flow rate setting range	0 ~ 100mL/min
Programmable Steps	7
Programmed rate setting range	-400 ~ 400mL/min
Correction Function	Maintains column flow rate during column oven heating
For Capillary Split/Splitless (Split/Splitless injection mode)
Pressure Setting Range	0 ~ 970kPa
Programmable Steps	7 (pressure-decreasing program possible)
Programmed rate setting range	-400 ~ 400kPa/min
Total flow rate setting range	0 ~ 200 mL/min
Correction Function	Maintains column average linear velocity during column oven heating (for capillary only)
(Pressure mode direct injection)
Pressure Setting Range	0 ~ 970kPa/min
Programmable Steps	7
Programmed rate setting range	-400 ~ 400kPa/min
(Flow-rate mode direct injection)
Flow rate setting range	0 ~ 1200mL/min
Programmable Steps	7
Programmed rate setting range	-400 ~ 400mL/min
Correction Function	Maintains column average linear velocity during column oven heating (for capillary only)

Detectors
Temperature Range	400°C max. (FID, TCD, FTD) 350°C max. (ECD, FPD)
Temperature Setting	1°C steps
No. of units installed simultaneously	Up to 4 units (restricted depending on detector type)
Detector Type	FID, TCD, ECD, FPD, FTD for capillary/packed
Flame Ionization Detector (FID)
System	Dual flow rate differential system
Temperature Range	400°C max.
Minimum detected quantity	3pgC/s (dodecane)
Dynamic Range	10⁷
Nozzle	Quartz glass Standard: for packed, Option: for capillary
Thermal Conductivity Detector (TCD)
System	Dual flow rate differential system
Temperature Range	400°C max.
Dynamic Range	10⁵
Sensitivity	40,000 mV - mL/mg (built-in pre-amplifier, with 10 x amplification)
Electron Capture Detector (ECD)
System	Fixed current system using ⁶³Ni370MBq radiation source
Temperature Range	400°C max.
Minimum detected quantity	0.1pg/s
Dynamic Range	10⁴
Flame Photometric Detector (FPD)
Temperature Range	350°C max.
Dynamic Range	P: 10⁴ S: 10³
Minimum detected quantity	P: 0.5pgP/s (tributyl phosphate) S: 8pgS/s (dodecane thiol)
Flame Thermionic Detector (FTD) (Two types, one for capillary and one for packed. The specifications are the same.)
Temperature Range	400°C max.
Dynamic Range	N: 10³ P: 10³
Minimum detected quantity	N: 0.4pgN/s (azobenzene) P: 8pgP/s (malathion)

Display
Dimensions	240 x 320 dot graphics display (30 characters x 16 lines)

Dimensions, Weight, Power Requirements (GC main unit)
Dimensions	400 (W) x 690 (H) x 607 (D) mm
Weight	48 kg (GC-2014AF model)
Power Requirements	AC100V/120V 230V 1800VA (GC-2014AF model) or 2600VA (GC-2014AF model), 50/60Hz